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Effect of heat treatment on crystal phase and photocatalytic activity of Tm doped TiO2 Nanoparticles.
作者:W. Y. Zhou, Q. Y. Cao, X. Y. Yu,J. L. Jia and Y. H. Xu
关键字:Nanosized titania, Tm doping, Hydrolysis precipitation method
论文来源:期刊
具体来源:Advances in Applied Ceramics 2010 VOL 109
发表时间:2010年

Tm doped TiO2 nanoparticles have been synthesised by hydrolysis–precipitation method. The effect of heat treatment on the crystal phase and photocatalytic activity of Tm doped TiO2 nanoparticles has been studied. The prepared samples were characterised by transmission electron microscopy, X-ray diffraction, Fourier transformed infrared and diffuse reflection spectrum analysis. The results show that Tm3z doping can effectively inhibit the phase transformation from antase to rutile and decrease the crystallite size of nano-TiO2 particles. There is an optimal Tm doping (1?4 mol.-%) after calcination at 550uC for the photocatalytic activity of methylene blue degradation.