writer:Yan Zhang, Linbo Wu, Feng Li and Bo-Geng Li
keywords:Altaicadispirolactone, 5-hydroxylevulinic acid, lactonization, levulinic acid
source:期刊
specific source:Synthetic Communications, 35(21): 2729-2733, 2005
Issue time:2005年
Altaicadispirolactone was synthesized via a simple route. In this route, levulinic acid was used as a starting material, and bromination followed by hydrolysis and BF3 . OEt2-catalyzed cyclization were carried out. A single-crystal ORTEP drawing has been created and more detailed crystallographic data of the compound has been obtained from X-ray analysis.